Data File D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\BIZ2016-226-WJ5.DSample Name: BIZ2016-226-WJ5=====================================================================Acq. Operator : Wang Ke Cheng(LCMS-02) Seq. Line : 57Acq. Instrument : HY-LCMS-02 Location : P1-C-01Injection Date : 2/26/2016 3:05:57 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 2/26/2016 9:17:10 AM by Wang Ke Cheng(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 2/26/2016 3:29:26 PM by Wang Ke Cheng(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-19725 Batch#195 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\BIZ2016-226-WJ5.D) 2.029 1.509 1.755 1.809 1.629 1.929 2.149mAU2000175015001250100075025000.51 2.2425001.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.509 MM 0.0405 14.27910 5.87686 0.2143 2 1.629 MM 0.0481 5.200 1.80511 0.0782 3 1.755 MF 0.04 9.79533 3.51568 0.1470 4 1.809 FM 0.0541 37.18509 11.46233 0.5579 5 1.929 MF 0.0466 31.808 11.31331 0.4749 6 2.029 MF 0.0520 6531.69580 2094.42529 98.0052 7 2.149 FM 0.0366 24.05917 10.95998 0.3610 8 2.242 MM 0.0392 10.76832 4.58405 0.1616 Totals : 66.63980 2143.94263 ===================================================================== *** End of Report ***HY-LCMS-02 2/26/2016 3:29:28 PM Wang Ke Cheng(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\BIZ2016-226-WJ5.DSample Name: BIZ2016-226-WJ5=====================================================================Acq. Operator : Wang Ke Cheng(LCMS-02) Seq. Line : 57Acq. Instrument : HY-LCMS-02 Location : P1-C-01Injection Date : 2/26/2016 3:05:57 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 2/26/2016 9:17:10 AM by Wang Ke Cheng(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 2/26/2016 3:24:17 PM by Wang Ke Cheng(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-19725 Batch#195 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\BIZ2016-226-WJ5.D) ES-API, Pos, Scan 2.0281600001400001200001000008000060000400002000000.511.522.53min HY-LCMS-02 2/26/2016 3:24:20 PM Wang Ke Cheng(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\BIZ2016-226-WJ5.DSample Name: BIZ2016-226-WJ5MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 2.028 695729 671.30 I 670.30 I 335.70 I 224.20 I*MSD1 SPC, time=1.999:2.054 of D:\\AGLIENT 1260\\DATA\\20160226\\20160226 2016-02-26 09-17-10\\BIZ2016-226-WJ5.D ES-API, 100806040200100200300400500600700m/z 224.2 671.3 670.3 335.7Max: 74134 *** End of Report ***HY-LCMS-02 2/26/2016 3:24:20 PM Wang Ke Cheng(LCMS-02)Page 2 of 2
