CC-115_LCMS_18566_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\BIZ2015-N16-WJ10.DSample Name: BIZ2015-N16-WJ10=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 62Acq. Instrument : HY-LCMS-02 Location : P1-E-08Injection Date : 11/16/2015 2:59:45 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.MLast changed : 11/16/2015 9:08:15 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20151110\\20151110 2015-11-10 11-24-47\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M (Sequence Method)Last changed : 11/16/2015 3:09:23 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-16962 Batch#18566 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...60\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\BIZ2015-N16-WJ10.D) 1.0 1.465 1.672 1.726 1.812mAU14001200100080060040020000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.465 MF 0.0463 113.95709 41.00590 2.5769 2 1.0 FM 0.0436 4201.326 1607.80029 95.0061 3 1.672 MF 0.0259 14.13288 9.10119 0.3196 4 1.726 FM 0.0458 84.60346 30.75382 1.9132 5 1.812 MM 0.0483 8.14911 2.65218 0.1843 Totals : 4422.20680 1691.31338 ===================================================================== *** End of Report ***HY-LCMS-02 11/16/2015 3:09:25 PM Yang Qian(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\BIZ2015-N16-WJ10.DSample Name: BIZ2015-N16-WJ10=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 62Acq. Instrument : HY-LCMS-02 Location : P1-E-08Injection Date : 11/16/2015 2:59:45 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.MLast changed : 11/16/2015 9:08:15 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20151110\\20151110 2015-11-10 11-24-47\\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.M (Sequence Method)Last changed : 11/16/2015 3:10:42 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-16962 Batch#18566 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\BIZ2015-N16-WJ10.D) ES-API, Pos, Sca 1.180000070000060000050000040000030000020000010000000.511.522.53min HY-LCMS-02 11/16/2015 3:10:44 PM Yang Qian(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\BIZ2015-N16-WJ10.DSample Name: BIZ2015-N16-WJ10MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.1 2791596 338.15 I 337.20 I*MSD1 SPC, time=1.525:1.562 of D:\\AGLIENT 1260\\DATA\\20151116\\20151116 2015-11-16 09-08-15\\BIZ2015-N16-WJ10.D ES-API,100806040200100200300400500600700800m/z 338.1 337.2Max: 5133 *** End of Report ***HY-LCMS-02 11/16/2015 3:10:44 PM Yang Qian(LCMS-02) 169.1Page 2 of 2