Method for the continuous synthesis of monoalkyl-h
专利名称:Method for the continuous synthesis of
monoalkyl-hydrazines with a functionalisedalkyl group
发明人:Henri Delalu,Cecile Colas-Duriche,Jacques
Berthet,Philippe Leurent
申请号:US10583285申请日:20041217
公开号:US20070185351A1公开日:20070809
专利附图:
摘要:The invention relates to a method for the continuous synthesis of monoalkyl-
hydrazines with a functionalised alkyl group. The inventive method is characterised in thatit comprises a step consisting in demixing a solution containing the synthesised
monoalkyl hydrazine, by reacting an anhydrous amine with monochloramine, in an organicphase and an aqueous phase with the addition of anhydrous sodium hydroxide. Theinvention can he used to obtain perfect selectivity in relation to monoalkyl-hydrazinewithout the presence of the di- and tri-substituted forms thereof. According to theinvention, the starting amine which has not reacted is collected and reused directlywithout any additional treatment.
申请人:Henri Delalu,Cecile Colas-Duriche,Jacques Berthet,Philippe Leurent
地址:Lyon FR,Talence FR,Lyon FR,Toulouse FR
国籍:FR,FR,FR,FR
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