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Method for the continuous synthesis of monoalkyl-h

来源:化拓教育网
专利内容由知识产权出版社提供

专利名称:Method for the continuous synthesis of

monoalkyl-hydrazines with a functionalisedalkyl group

发明人:Henri Delalu,Cecile Colas-Duriche,Jacques

Berthet,Philippe Leurent

申请号:US10583285申请日:20041217

公开号:US20070185351A1公开日:20070809

专利附图:

摘要:The invention relates to a method for the continuous synthesis of monoalkyl-

hydrazines with a functionalised alkyl group. The inventive method is characterised in thatit comprises a step consisting in demixing a solution containing the synthesised

monoalkyl hydrazine, by reacting an anhydrous amine with monochloramine, in an organicphase and an aqueous phase with the addition of anhydrous sodium hydroxide. Theinvention can he used to obtain perfect selectivity in relation to monoalkyl-hydrazinewithout the presence of the di- and tri-substituted forms thereof. According to theinvention, the starting amine which has not reacted is collected and reused directlywithout any additional treatment.

申请人:Henri Delalu,Cecile Colas-Duriche,Jacques Berthet,Philippe Leurent

地址:Lyon FR,Talence FR,Lyon FR,Toulouse FR

国籍:FR,FR,FR,FR

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