1.平衡釜操作记录实验时间:3h57min 室温:25.83 大气压: 100.05KPa 平衡釜温冷凝液滴釜加热电压(V)投料量时间现象备注度(℃)速(滴/开始加热12:24102026.0012:27152526.0012:30203026.10沸腾器内开始有气泡12:33253526.7012:36304027.60气泡大量上升12:39354529.20开始沸腾12:42405032.8012:45455544.4012:48506053.50沸腾厉害,偶尔有大气泡12:51506058.80出现第一滴液体,气泡变密12:54506061.70混合液13:305060.50200ml:……140ml14:584657.283环己烷15:034657.284+ 60ml15:084657.283乙醇15:134657.27515:184657.27715:234657.27515:284657.280液滴速度趋于稳定,沸腾器提取样品1中的原料沸腾剧烈,气泡夹……带液滴,温度基本稳定15:514657.27815:5657.28516:014657.27616:0657.27516:114657.28516:1657.285提取样品216:214657.2752.折光系数测定及数据计算结果
测量温度 30.0℃原料样品折光系数12341.39681.39691.39701.3970样品1折光系数1液相1.3968气相1.3970样品2折光系数1液相1.3970气相1.3971平均1.396921.39681.397031.39701.397041.39701.3968平均1.39691.3970平衡组成0.48130.480521.39701.397031.39711.397041.39691.3970平均1.39701.3970平衡组成0.47970.4793